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Journal of Dairy Science Vol. 44 No. 6 1036-1046
© 1961 by American Dairy Science Association ®
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Determination of Calcium and Magnesium in Milk by E.D.T.A. Titration1

E. W. Bird and June Weber

Department of Dairy and Food Industry

C. P. Cox2 and T. C. Chen3

Department of Statistics Iowa State University, Ames, Iowa

ABSTRACT

Five procedures were compared for E.D.T.A. determination of calcium and magnesium in milk. The method which combined Ling's method for removal of proteins and phosphates by potassium metastannate, Flashka's indicator (Eriochrome blue S E) for the calcium determination, his adjustment of pH in the magnesium determination, and the method of Jenness (slightly modified) for magnesium yielded the best results. The method is convenient, rapid, and recoveries for both calcium and magnesium were essentially 100%.


FOOTNOTES

1 Journal Paper No. J-3935 of the Iowa Agricultural Experiment Station, Ames, Project No. 1298.

2 Visiting Professor from the National Institute for Research in Dairying, University of Reading, England.

3 Current address: C. D. Searle and Co., Division of Biological Research, Chicago, Ill.







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